Thermo-FTIR spectroscopy analysis as a method of characterizing ancient ceramic technology

S. Shoval, P. Beck

Research output: Contribution to journalArticlepeer-review

Abstract

The Iron Age ceramic technology used in the manufacturing of cooking pots was studied by thermo-FTIR spectroscopy analysis. The pottery was excavated at Tel Hadar on the eastern shore of the Sea of Galilee. The results demonstrate that the cooking pots were manufactured using noncalcareous or slightly calcareous raw material proceeds from soil. The firing was at about 750-850°C and the cementation to ceramic was obtained by low temperature sintering of the clay. The use of soil raw material composed of smectitic (montmorillonitic) clay enabled the low temperature sintering. The clay from soil is relatively poorly crystallized and rich in natural iron oxide, both of which induce earlier sintering. Most of the cooking pots were tempered with broken pieces of large calcite crystals that were added to the clayey raw material from an additional source. Alternative tempering with limestone particles composed of polycrystalline calcite is inappropriate as it brings about earlier and intense decarbonation during the firing, which causes defects in the pots.

Original languageEnglish
Pages (from-to)609-616
Number of pages8
JournalJournal of Thermal Analysis and Calorimetry
Volume82
Issue number3
DOIs
StatePublished - Nov 2005

Bibliographical note

Funding Information:
This research was supported by the Israel Science Foundation administered by the Israel Academy of Sciences and Humanities and completed through the support of the Open University of Israel Research Authority. Both are gratefully acknowledged.

Keywords

  • Cooking pots
  • Firing
  • Infrared spectroscopy
  • Iron Age
  • Pottery raw material
  • Sintering
  • Tel-Hadar excavations
  • Temper

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